Emerald Weapon is memorable to me because of how challenging it was. I didn't look up guides for it back then. The Midgar Zolom is also fun to challenge at a lower level, and satisfying if you beat it. That one crane boss when you attempt to steal a sub is fun because it takes characters out of the battle briefly and adds challenge that usually isn't present. And for pure atmosphere, both final battles are just plain awesome.
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